LAP Lambert Academic Publishing ( 2019-10-30 )
€ 93,90
All reactions were carried out in oven dried glass wares. Reactions requiring inert atmosphere were carried out under nitrogen atmosphere. Dry THF was distilled as needed from Na/benzophenone ketyl. All anhydrous solvents were prepared according to standard procedures. Solvents used for chromatography were LR grade. Thin-layer chromatography was performed on aluminum plates coated with silica gel 60. Visualization was observed by UV light irradiation or by dipping into (Hanessian′s stain) a solution of cerium (IV) sulfate (2.5 g) and ammonium molybdate (6.25 g) in 10% sulfuric acid (250 mL) followed by charring on a hot plate. For olefins, permanganate stain was used (3 g potassium permanganate, 20 g potassium carbonate, 5 mL 5% sodium hydroxide, 300 mL water). For aldehydes, 2,4-DNP stain prepared by dissolving 6 g of 2, 4-dinitrophenylhydrazine in 30 mL of sulfuric acid and 40 mL of water in 100 mL of 95% ethanol was used.
Book Details: |
|
ISBN-13: |
978-620-2-07986-0 |
ISBN-10: |
620207986X |
EAN: |
9786202079860 |
Book language: |
English |
By (author) : |
Sudarsan Reddy Kasireddy |
Number of pages: |
384 |
Published on: |
2019-10-30 |
Category: |
Chemistry |